1. Inorganic Chemistry and Catalysis Group, Debye Institute for NanoMaterials Science, Utrecht University, Sorbonnelaan 16, 3584 CA Utrecht, The Netherlands, Department of Chemistry, University College London, 20 Gordon Street, London WC1H 0AJ, Department of Crystallography, Industrial Materials Group, Birkbeck College, University of London, London WC1E 7HX, U.K., and The European Synchrotron Facility, 6 Rue Jules Horowitz, BP220, 38043, Grenoble, CEDEX 9, France