1. Department of Inorganic, Materials and Physical Chemistry, Torino University, Via P. Giuria 7, I-10125 Turin, Italy, INSTM Unità di Torino Università, Turin, Italy, NIS Centre of Excellence, Università di Torino, Italy, ESRF, 6 rue Jules Horowitz, BP220, F-38043, Grenoble Cedex, France, Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin, BP48, F-91192 Gif sur Yvette Cedex, France