1. Department of Biochemical and Chemical Engineering, Laboratory of Thermodynamics, TU Dortmund University, Emil-Figge-Str. 70, Dortmund D-44227, Germany
2. Department of Chemical Sciences, SSPC the Science Foundation Ireland Research Centre for Pharmaceuticals, Bernal Institute, University of Limerick, Limerick V94 T9PX, Ireland
3. Janssen Research & Development, A Division of Janssen Pharmaceutica NV, Turnhoutsweg 30, Beerse 2340, Belgium