Investigation of Mechanochemical Sonogashira Couplings─From Batch Solution to Continuous Reactive Extrusion through Ball-Milling Optimization

Author:

Hastings Riley H.1ORCID,Mokhtar Mennatullah M.2,Ruggles Alexander3,Schmidt Constanze3,Bourdeau David1,Haibach Michael C.4ORCID,Geneste Hervé5,Mack James2,Co Sarah S.1,Speight Isaiah R.1ORCID

Affiliation:

1. Operations, Science and Technology, AbbVie, Inc., 1 North Waukegan Road, North Chicago, Illinois 60064, United States

2. Department of Chemistry, University of Cincinnati, 301 Clifton Court, Cincinnati, Ohio 45221, United States

3. Drug Product Development, AbbVie Inc., 1 North Waukegan Road, North Chicago, Illinois 60064, United States

4. Process Research & Development, AbbVie Inc., 1 North Waukegan Road, North Chicago, Illinois 60064, United States

5. AbbVie Deutschland GmbH & Co. KG, SMTPT, Knollstrasse, Ludwigshafen 67061, Germany

Funder

Division of Chemistry

AbbVie

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

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