Synthesis of Methyl 3-Hydroxyisoxazole-5-Carboxylate Via Bromination of Dimethyl Fumarate under Photoflow Conditions and Its Safe Homologation into 3-(3-Methoxyisoxazol-5-yl) Propanoic Acid
Author:
Affiliation:
1. Chemistry Process R&D, Idorsia Pharmaceuticals Ltd., Hegenheimermattweg 91, CH-4123 Allschwil, Switzerland
2. Pharmablock Sciences, 10 Xuefu Road, Jiangbei New Area, 210032 Nanjing, Jiangsu, P.R. China
Publisher
American Chemical Society (ACS)
Subject
Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/acs.oprd.3c00334
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1. Process Research and Development of an Enantiomerically Enriched Allyic Amine, One of the Key Intermediates for the Manufacture of Synthetic Tetracyclines
2. Explosive Hazard Identification in Pharmaceutical Process Development: A Novel Screening Method and Workflow for Shipping Potentially Explosive Materials
3. Use of Bromine and Bromo-Organic Compounds in Organic Synthesis
4. Electrophilic Bromination of Alkenes: Environmental, Health and Safety Aspects of New Alternative Methods
5. Identification of highly potent and orally available free fatty acid receptor 1 agonists bearing isoxazole scaffold
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