1. Department of Applied Chemistry, Tokyo University of Science, 1-3, Kagurazaka, Shinjuku, Tokyo 162-8601, Japan, Center for Marine Environmental Studies (CMES), Ehime University, Bunkyo-cho, Matsuyama-shi, Ehime 790-8577, Japan, and SPring-8, JASRI, 1-1-1, Kouto, Mikazuki-cho, Sayo-gun, Hyogo 679-5198, Japan