Total Synthesis of (+)-Calyculin A and (−)-Calyculin B: Cyanotetraene Construction, Asymmetric Synthesis of the C(26−37) Oxazole, Fragment Assembly, and Final Elaboration
Author:
Affiliation:
1. Contribution from the Department of Chemistry, the Laboratory for Research on the Structure of Matter, and the Monell Chemical Senses Center, University of Pennsylvania, Philadelphia, Pennsylvania 19104
Publisher
American Chemical Society (ACS)
Subject
Colloid and Surface Chemistry,Biochemistry,General Chemistry,Catalysis
Link
https://pubs.acs.org/doi/pdf/10.1021/ja992135e
Reference46 articles.
1. Absolute Stereochemistry of the Calyculins, Potent Inhibitors of Protein Phosphatases 1 and 2A
2. Total Synthesis of (+)-Calyculin A and (−)-Calyculin B
3. Calyculins E, F, G, and H, additional inhibitors of protein phosphatases 1 and 2a, from the marine sponge discodermia calyx
4. The Stereoselective Synthesis of α,β-Unsaturated Ketones by the Stepwise Cross-Coupling Reaction of [E]-(2-Bromoethenyl)diisopropoxyborane
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