1. Department of Chemistry, University of Oxford, Inorganic Chemistry Laboratory, South Parks Road, Oxford OX1 3QR, U.K.
2. EMAT, University of Antwerp, Groenenborgerlaan 171, Antwerp B-2020, Belgium
3. ISIS Facility, Rutherford Appleton Laboratory, Chilton ,Oxon OX11 0QX, U.K.