Optimization and Scale-Up of a Suzuki−Miyaura Coupling Reaction: Development of an Efficient Palladium Removal Technique
Author:
Affiliation:
1. Chemical Development, GlaxoSmithKline, Five Moore Drive, P.O. Box 13398, Research Triangle Park, North Carolina 27709, U.S.A.
Publisher
American Chemical Society (ACS)
Subject
Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/op800064y
Reference14 articles.
1. Generation of Tertiary Phosphine-Coordinated Pd(0) Species from Pd(OAc)2in the Catalytic Heck Reaction
2. Palladium-Catalyzed Cross-Coupling Reactions of Organoboron Compounds
3. High-Turnover Palladium Catalysts in Cross-Coupling and Heck Chemistry: A Critical Overview
4. dNote: consideration was also given to solvent selection based upon principal component analysis (PCA) diversity and boiling point of the solvent.
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