Structure of Galactosylononitol

Author:

Richter Andreas1,Peterbauer Thomas1,Brereton Ian2

Affiliation:

1. Institute of Plant Physiology, University of Vienna, A-1091 Vienna, Austria

2. Centre of Magnetic Resonance, University of Queensland, St. Lucia 4072, Australia

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Complementary and alternative medicine,Drug Discovery,Pharmaceutical Science,Pharmacology,Molecular Medicine,Analytical Chemistry

Reference16 articles.

1. Seed desiccation tolerance and storability: Dependence on flatulence-producing oligosaccharides and cyclitols—review and survey

2. Synthesis of specifically fluorinated methyl β-glycosides of (1→6)-β-d-galacto-oligosaccharides

3. 2D NMR spectra were for D2O solutions measured on a Bruker DRX500 spectrometer operating at 500.1 MHz (1H) or 125.75 MHz (13C).1H and13C chemical shifts are measured relative to TSP-d6(sodium (trimethylsilyl)propionate) internal standard. Phase-sensitive NOESY (tm= 800 ms) and DQF-COSY spectra15were typically acquired with a spectral width of 4 ppm in each dimension using a 1024 × 256 complex data matrix. The data were zero-filled to give a final data matrix of 2048 × 512 complex points, and a 90°-shifted sine-squared function was applied prior to Fourier transformation in each dimension. The gradient-enhanced HSQC16and HMBC17spectra were acquired with spectral widths of 4 and 60 ppm in the1H and13C dimensions, respectively, using a 1024 × 256 complex data matrix and were processed as described for the DQF−COSY spectra.

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