1. Department of Inorganic Chemistry and Catalysis, Debye Institute, Utrecht University, Sorbonnelaan 16, 3584 CA Utrecht, The Netherlands, DUBBLE CRG, ESRF, BP 220, 38043 Grenoble Cedex 9, France, and Material Engineering Division, Toyota Motor Engineering & Manufacturing Europe Technical Centre, Hoge Wei 33B, B-1930 Zaventem, Belgium