1. Department of Physics and Earth Sciences, University of Ferrara, via Saragat 1, I-44121 Ferrara, Italy
2. European Synchrotron CS40220, Grenoble Cedex 9, F-38043 Grenoble, France
3. Department of Environmental and Prevention Sciences, University of Ferrara, via Borsari 46, I-44121 Ferrara, Italy