Use of a Titanium Thienyl Anion and a Simple Procedure for Introducing a Thiol Group into Thiophene in the Development of a Manufacturing Route to the 5-Lipoxygenase Inhibitor ZD4407
Author:
Affiliation:
1. Process Development Department, ZENECA Pharmaceuticals, Hurdsfield Industrial Estate, Macclesfield, Cheshire SK10 2NA, U.K.
Publisher
American Chemical Society (ACS)
Subject
Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/op960029g
Reference8 articles.
1. Base-catalyzed halogen dance reaction at thiophenes: a spectroscopic reinvestigation of the synthesis of 2,5-dibromo-3-(trimethylsilyl)thiophene
2. Bretherick'sHandbookofReactiveChemicalHazards; Butterworth-Heinemann Ltd: Oxford, 1992; p 1181 and references cited therein.
3. Room temperature stable 3-lithiothiophene: a facile synthesis of 3-functional thiophenes
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