1. Chemistry Department, Brookhaven National Laboratory, Upton, New York 11973, Mineral Physics Institute & Department of Geosciences, Stony Brook University, Stony Brook, New York 11794, University of Tennessee, Knoxville, Tennessee 37996, Instrumentation Division, Brookhaven National Laboratory, Upton, New York 11973, and Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, New York 11973