Heavy-Metal-Free Reduction Methodology for Large-Scale Synthesis Applicable to Heterocyclic and Arylhydrazines-Reference-Cited by-同舟云学术

Heavy-Metal-Free Reduction Methodology for Large-Scale Synthesis Applicable to Heterocyclic and Arylhydrazines

Published:2008-12-12 Issue:2 Volume:13 Page:354-357
ISSN:1083-6160
Container-title:Organic Process Research & Development
language:en
Short-container-title:Org. Process Res. Dev.

Author:

Norris Timothy¹,Bezze Chiara¹,Franz Samuela Zambelli¹,Stivanello Mariano¹

Affiliation:

1. Chemical Research and Development, Pfizer Inc., Global Research and Development Laboratories, Eastern Point Road, Groton, Connecticut 06340, U.S.A.

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/op8002163

Reference12 articles.

1. Lambert, J. F. and Norris, T.Preparation of Sodium-Hydrogen Exchanger Type I Inhibitors. Patent Application WO 02/44133 A1, 2002.

2. LXX.—The hydrazines of quinoline

3. Über die Einwirkung von Diazoniumsalzen auf Ascorbinsäure; eine allgemeine Reaktion von Dienolen

4. 1H NMR (DMSO-d6) δ 7.94 (broad s, 1H), 7.76 (d,J= 8.6 Hz, 1H), 7.67 (dd,J= 2.5,J= 8.6 Hz, 1H), 7.41 (d,J= 2.5 Hz, 1H), 7.12 (broad s, 1H), 5.67 (broad s, 1H), 4.64 (s, 1H), 4.40 (dd,J= 3.7 Hz,J= 6.0 Hz, 1H), 4.26 (dd,J= 6.0 Hz,J= 9.5 Hz, 1H), 3.96 (dd,J= 3.7 Hz,J= 9.5 Hz, 1H).

5. See ref3, p 2017.

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