1. Department of Chemistry, The University of Tennessee, Knoxville, Tennessee 37996, United States
2. Chemical and Engineering Materials Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37830, United States
3. ChemMatCARS,
Center for Advanced Radiation Sources, The University of Chicago, Argonne, Illinois 60439, United States
4. Institut Laue-Langevin, BP 156, 38042 Grenoble Cedex 9, France