1. National Institute of Agrobiological Sciences, 2-1-2 Kannondai, Tsukuba, Ibaraki 305-8602, Japan; National Food Research Institute, 2-1-2 Kannondai, Tsukuba, Ibaraki 305-8642, Japan; ESR Application and Research Center, Analytical Instrument Division, JOWL Ltd., 1-2 Musashino 3 Chome, Akishima, Tokyo 196-8558, Japan; and National Agricultural Research Center for Kyushu Okinawa Region, 2421 Suya, Nishigoushi, Kikuchi, Kumamoto 861-1192, Japan