Synthesis of new fluorene-containing 9-azabicyclo[4.2.1]nona-2,4,7-trienes [6π+2π]-cycloaddition of alkynes to <i>N</i>-carbofluorenylmethoxyazepine-Reference-Cited by-同舟云学术

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Synthesis of new fluorene-containing 9-azabicyclo[4.2.1]nona-2,4,7-trienes [6π+2π]-cycloaddition of alkynes to <i>N</i>-carbofluorenylmethoxyazepine

Published:2023-06-15 Issue:6 Volume:59 Page:807-814
ISSN:0514-7492
Container-title:Журнал органической химии
language:
Short-container-title:Žurnal organičeskoj himii

Author:

Kadikova G. N¹,D'yakonov V. A²

Affiliation:

1. Institute of Petrochemistry and Catalysis, Ufa Federal Research Center, Russian Academy of Sciences

2. N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences

Abstract

Catalytic [6π+2π]-cycloaddition of terminal alkynes to N -carbofluorenylmethoxyazepine under the action of a three-component catalytic system Co(acac)2(dppe)/Zn/ZnI2 was performed for the first time to obtain previously undescribed and promising 9-azabicyclo[4.2.1]nona-2,4,7-trienes (in 79-92% yields) containing a fluorene substituent.

Publisher

The Russian Academy of Sciences

Reference52 articles.

1. 9-Azabicyclo[4.2.1]nona-2,4,7-triene and derivatives

2. The question of the reversibility in the aminomercuration of olefins. Synthesis of N-aryl-9-azabicyclo[4.2.1]and [3.3.1] nonanes by aminomercuration of cis-cis- 1.5-cyclooctadiene

3. Efficient new syntheses of (+)- and (-)-anatoxin-a. Revised configuration of resolved 9-methyl-9-azabicyclo[4.2.1]nonan-2-one

4. Synthesis and Nicotinic Binding Studies on Enantiopure Diazine Analogues of the Novel (2-Chloro-5-pyridyl)-9-azabicyclo[4.2.1]non-2-ene UB-165

5. Application of Intramolecular Enyne Metathesis to the Synthesis of Aza[4.2.1]bicyclics: Enantiospecific Total Synthesis of (+)-Anatoxin-a

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