"2+1" Technetium and Rhenium Tricarbonyl Complexes with <i>N</i>,<i>N</i>′-Bidentate Ligands and Methyl 11-Isocyanoundecanoate

Author:

Miroslavov A. E123,Sakhonenkova A. P123,Tyupina M. Yu.134,Sidorenko G. V1

Affiliation:

1. Khlopin Radium Institute

2. St. Petersburg State University

3. Ozersk Technological Institute of the National Research Nuclear University

4. St. Petersburg State Pediatric Medical University

Abstract

«2+1» tricarbonyl complexes [M(CO)3(N^N)CN(CH2)10COOMe]ClO4, where M = Tc or Re and N^N = 2,2′-bipridine (bipy) or 1,10-phernanthroline (phen), were prepared by reaction of [M(CO)3(N^N)(MeOH)]ClO4 with methyl 11-isocyanoundecanoate in methanol. The complexes were isolated and characterized by IR, 1H NMR spectroscopy and elemental analysis. Stability of the «2+1» tricarbolyl complexes with respect to transchelation with histidine was studied.

Publisher

The Russian Academy of Sciences

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