A correlation between Bogue's equations and Taylor's procedure for the evaluation of crystalline phases in special class Portland oilwell cement clinker

Author:

Bezerra U. T.1,Martinelli A. E.2,Melo D. M. A.2,Melo M. A. F.2,Lima F. M.3

Affiliation:

1. Federal Centre of Tech. Education of Paraíba

2. Federal University of Rio Grande do Norte

3. Petróleo Brasileiro S.A.

Abstract

The crystalline composition of Portland cement clinker is commonly established by Bogue's equations, which are based on a series of assumptions that seldom apply to oilwell cements. This is probably due to the presence of additional oxides and phase reconversion upon cooling of the clinker from the calcination temperature. Important differences are therefore observed between the numerical values yielded by the mathematical equations and image analysis quantification. In this study, the concentration of crystalline phases in oilwell cement was determined using Taylor's procedure, which consists in a system of linear equations corresponding to each one of the four main clinker phases. The results revealed an adequate relationship between this method and phase quantification by optical micrography, especially concerning the contents of aluminate and ferrite.

Publisher

FapUNIFESP (SciELO)

Subject

Ceramics and Composites

Reference15 articles.

1. Desenvolvimento de concretos duráveis e resistentes através do uso de cinzas volantes e escória de alto forno moída;Swamy R. N.,1998

2. O efeito de adições minerais nas propriedades mecânicas de pastas de cimento Portland reforçadas com fibras de polipropileno;Morelli A. C.,2001

3. Standard Test Method for Quantitative Determination of Phases in Portland Cement Clinker by Microscopical Point-Count Procedure 1,2001

4. Concrete: microstructure, properties and materials;Mehta P. K.,2005

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