Author:
Alduhaileb Raed A.,Ayres Virginia M.,Jacobs Benjamin W.,Fan Xudong,McElroy Kaylee,Crimp Martin,Hirata Atsushi,Horikoshi Mutsumi
Abstract
AbstractThe evolution of carbon onion structure from spherical to polyhedral is correlated with changes in the sp3/sp2 ratio as a function of increasing synthesis temperature using electron energy loss spectroscopy, scanning electron microscopy, and high resolution electron microscopy. Results that are obtained using asymmetric f-variance versus symmetric Gaussian deconvolution of electron energy loss spectra are compared. The possibility of a separate peak at 287 eV is discussed.
Publisher
Springer Science and Business Media LLC