Author:
Cao X.,Koltypin Yu,Kataby G.,Prozorov R.,Gedanken A.
Abstract
A method for controlling the particle size of amorphous iron, which was prepared by the sonication of iron pentacarbonyl [Fe(CO)5], is reported in this paper. The sonolysis was performed on neat Fe(CO)5 and its solutions in decane whose concentrations were 4 M, 1 M, and 0.25 M. The iron nanoparticles were subjected to TEM (Transmission Electron Micrograph), ESR (Electron Spin Resonance), TGA (Thermogravimetric Analysis), DSC (Differential Scanning Calorimctry), and Quantum Design SQUID magnetization measurement. The measured properties demonstrated a strong dependence on the concentration of the solution, e.g., particle size.
Publisher
Springer Science and Business Media LLC
Subject
Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science
Cited by
72 articles.
订阅此论文施引文献
订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献