Applications of Reactive Gas Plasma Cleaning Technology in Minimizing Contamination Of Specimens During Transmission and Analytical Electron Microscopy

Author:

Roberts S. P.,Zaluzec N. J.,Walck S. D.,Grant J. T.

Abstract

AbstractThe generation and usage of a reactive gas plasma for a wide range of applications has been cited since the early 1970's. More recently, the use of a plasma generating system has been applied to analytical transmission electron microscopy to minimize and, in some cases, eliminate the problems associated with various contamination sources, including the specimen holder and the specimen itself. Although the technology is well known, no definitive characterization of process parameters has been developed for specimen and specimen holder cleaning applications. An investigation of the effects that power levels and gas mixtures have upon contamination rates and removal were done using a Philips CM30T. Measurements of contamination rates both prior to and following plasma cleaning were done to characterize the effects of various parameter changes. Results of different process parameters and contamination rates will be reported.

Publisher

Springer Science and Business Media LLC

Subject

General Engineering

Reference5 articles.

1. 1. Brundle C. , Evans C. Jr. , Encyclopedia of Materials Characterization, Reed Publishing, (1992), Chptr. 3.0, 5.1.

2. 2. Hren J.J. , Introduction to Analytical Electron Microscopy Plenum Press, (1979), Chptr. 18.

3. 3. Simultaneous Specimen and Stage Cleaning Device for Analytical Electron Microscopy, US Patent # 5,510,624- Argonne National Laboratory and the University of Chicago.

4. 4. Williams D. , Carter C. Barry , Transmission Electron Microscopy: Spectrometry. Plenum Publishing, (1996), Chptr. 32.

5. 5. Surface Science Aspects of Contamination in TEM Sample Preparation, Grant John T. , Walck Scott D. , Scheltens Frank J. , and Voevodin Andrey A. , these Proceedings of the Spring 1997 Materials Research Society Meeting, San Francisco, CA, 1997

Cited by 8 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

同舟云学术

1.学者识别学者识别

2.学术分析学术分析

3.人才评估人才评估

"同舟云学术"是以全球学者为主线,采集、加工和组织学术论文而形成的新型学术文献查询和分析系统,可以对全球学者进行文献检索和人才价值评估。用户可以通过关注某些学科领域的顶尖人物而持续追踪该领域的学科进展和研究前沿。经过近期的数据扩容,当前同舟云学术共收录了国内外主流学术期刊6万余种,收集的期刊论文及会议论文总量共计约1.5亿篇,并以每天添加12000余篇中外论文的速度递增。我们也可以为用户提供个性化、定制化的学者数据。欢迎来电咨询!咨询电话:010-8811{复制后删除}0370

www.globalauthorid.com

TOP

Copyright © 2019-2024 北京同舟云网络信息技术有限公司
京公网安备11010802033243号  京ICP备18003416号-3