Sans Measurement of Deuterium-Dislocation Correlation in Palladium

Author:

Heuser Brent J.,Summerfield G.C.,King J.S.,Epperson J.E.

Abstract

ABSTRACTSmall angle neutron scattering (SANS) measurements have been made on deformed polycrystal palladium samples with and without deuterium dissolved in the solution phase (a) at room temperature. Concentrations were held constant during SANS experiments by an equilibrium gas pressure cell. The difference scattering cross section for the same sample with and without deuterium loading has a 1/Q behavior (Q=4Φ/λsinθ/2) at intermediate values of Q. At very low values of Q the dependence is much stronger than 1/Q. The 1/Q behavior is attributed to deuterium trapping close to long dislocation cores forming rod-like scattering structures.

Publisher

Springer Science and Business Media LLC

Subject

General Engineering

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3. The effect of the α-β phase change on the α phase solubility of hydrogen in palladium

4. Small Angle Scattering of Subthermal Neutrons from Deformed Polycrystalline Copper

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