5′-Oxospiro-(fluorene-9,4′-imidazolidine)-2′-thione

Author:

Stoitsov Dimitar1ORCID,Marinov Marin2,Penchev Plamen1ORCID,Marinova Petya3ORCID,Stoyanov Neyko4

Affiliation:

1. Department of Analytical Chemistry and Computer Chemistry, Faculty of Chemistry, University of Plovdiv, “Tzar Asen” Str. 24, 4000 Plovdiv, Bulgaria

2. Department of Chemistry and Phytopharmacy, Faculty of Plant Protection and Agroecology, Agricultural University-Plovdiv, 4000 Plovdiv, Bulgaria

3. Department of General and Inorganic Chemistry with Methodology of Chemistry Education, Faculty of Chemistry, University of Plovdiv, “Tzar Assen” Str. 24, 4000 Plovdiv, Bulgaria

4. Department of Chemical, Food and Biotechnologies, “Angel Kanchev” University of Ruse, Razgrad Branch, 7200 Razgrad, Bulgaria

Abstract

The structure verification of 5′-oxospiro-(fluorene-9,4′-imidazolidine)-2′-thione by NMR is reported. Toward this aim, 2D NMR techniques including 1H-1H COSY, HMQC, and HMBC experiments were used to assist with the assignment of the 1H and 13C chemical shifts for the corresponding structure. The mutual interpretation of the 1D and 2D NMR spectra ensured a complete and accurate 1H and 13C NMR data assignment for 5′-oxospiro-(fluorene-9,4′-imidazolidine)-2′-thione.

Funder

Fund for Scientific Research of Plovdiv University

Publisher

MDPI AG

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