Development and Validation of LC-MS/MS Method for the Determination of 1-Methyl-4-Nitrosopiperazine (MNP) in Multicomponent Products with Rifampicin—Analytical Challenges and Degradation Studies
Author:
Affiliation:
1. Spectrometric Methods Department, National Medicines Institute, 30/34 Chełmska, 00-725 Warsaw, Poland
2. Department of Drug Chemistry, Doctoral School, Medical University of Warsaw, 61 Żwirki i Wigury, 02-091 Warsaw, Poland
Abstract
Funder
Polish Ministry of Health
Publisher
MDPI AG
Subject
Chemistry (miscellaneous),Analytical Chemistry,Organic Chemistry,Physical and Theoretical Chemistry,Molecular Medicine,Drug Discovery,Pharmaceutical Science
Link
https://www.mdpi.com/1420-3049/28/21/7405/pdf
Reference43 articles.
1. (2021, May 13). Potential Dangers of Nitrosamines in Rifampin and Rifapentine. Available online: https://www.adamsonlab.com/potential-dangers-of-nitrosamines-in-rifampin-and-rifapentine/.
2. Evolution of Rifampicin Treatment for Tuberculosis;Grobbelaar;Infect. Genet. Evol.,2019
3. Beloor Suresh, A., Rosani, A., and Wadhwa, R. (2023). Rifampin, StatPearls Publishing.
4. Rifampin vs. Rifapentine: What Is the Preferred Rifamycin for Tuberculosis?;Alfarisi;Expert Rev. Clin. Pharmacol.,2017
5. Critical Analysis of Drug Product Recalls Due to Nitrosamine Impurities;Bharate;J. Med. Chem.,2021
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