Effect of Plasma Treatment on Bamboo Fiber-Reinforced Epoxy Composites

Author:

Rachtanapun Pornchai1ORCID,Sawangrat Choncharoen2ORCID,Kanthiya Thidarat3,Thipchai Parichat4,Kaewapai Kannikar5,Suhr Jonghwan6ORCID,Worajittiphon Patnarin7ORCID,Tanadchangsaeng Nuttapol8ORCID,Wattanachai Pitiwat9,Jantanasakulwong Kittisak13

Affiliation:

1. Faculty of Agro-Industry, Chiang Mai University, Chiang Mai 50100, Thailand

2. Department of Industrial Engineering, Faculty of Engineering, Chiang Mai University, Chiang Mai 50200, Thailand

3. Office of Research Administration, Chiang Mai University, Chiang Mai 50200, Thailand

4. Nanoscience and Nanotechnology, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

5. Science and Technology Park (STeP), Chiang Mai University, Chiang Mai 50100, Thailand

6. School of Mechanical Engineering, Sungkyunkwan University, 2066 Seobu-ro, Jangan-gu, Suwon-si 16419, Gyeonggi-do, Republic of Korea

7. Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai 50200, Thailand

8. College of Biomedical Engineering, Rangsit University, Pathumthani 12000, Thailand

9. Department of Civil Engineering, Faculty of Engineering, Chiang Mai University, Chiang Mai 50200, Thailand

Abstract

Bamboo cellulose fiber (BF)-reinforced epoxy (EP) composites were fabricated with BF subjected to plasma treatment using argon (Ar), oxygen (O2), and nitrogen (N2) gases. Optimal mechanical properties of the EP/BF composites were achieved with BFs subjected to 30 min of plasma treatment using Ar. This is because Ar gas improved the plasma electron density, surface polarity, and BF roughness. Flexural strength and flexural modulus increased with O2 plasma treatment. Scanning electron microscopy images showed that the etching of the fiber surface with Ar gas improved interfacial adhesion. The water contact angle and surface tension of the EP/BF composite improved after 10 min of Ar treatment, owing to the compatibility between the BFs and the EP matrix. The Fourier transform infrared spectroscopy results confirmed a reduction in lignin after treatment and the formation of new peaks at 1736 cm−1, which indicated a reaction between epoxy groups of the EP and carbon in the BF backbone. This reaction improved the compatibility, mechanical properties, and water resistance of the composites.

Funder

NSRF via the Program Management Unit for Human Resources and Institutional Development, Research, and Innovation

Publisher

MDPI AG

Reference64 articles.

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