How Retting Could Affect the Mechanical Behavior of Flax/Epoxy Biocomposite Materials?

Author:

Ragoubi Mohamed1ORCID,Lecoublet Morgan1,Khennache Mehdi1,Atanase Leonard Ionut23ORCID,Poilane Christophe4,Leblanc Nathalie1ORCID

Affiliation:

1. UniLaSalle, Unité de Recherche Transformation et Agro-Ressources, VAM2IN (ULR 7519 UniLaSalle—Université d’Artois), 76130 Mont-Saint-Aignan, France

2. Faculty of Medical Dentistry, Apollonia University of Iasi, 700511 Iasi, Romania

3. Academy of Romanian Scientists, 050045 Bucharest, Romania

4. Normandie Université, Université de Caen Normandie (UNICAEN), 14000 Caen, France

Abstract

This study focuses on the retting effect on the mechanical properties of flax biobased materials. For the technical fiber, a direct link was established between the biochemical alteration of technical flax and their mechanical properties. In function of the retting level, technical fibers appeared smoother and more individualized; nevertheless, a decrease in the ultimate modulus and maximum stress was recorded. A biochemical alteration was observed as the retting increased (a decrease in the soluble fraction from 10.4 ± 0.2 to 4.5 ± 1.2% and an increase in the holocellulose fractions). Regarding the mechanical behavior of biocomposites manufactured by thermocompression, a non-elastic behavior was observed for the tested samples. Young moduli (E1 and E2) gradually increased with retting. The retting effect was more pronounced when a normalization was performed (according to the fiber volume and porosity). A 40% increase in elastic modulus could be observed between under-retting (−) and over-retting (+). Moreover, the porosity content (Vp) increased overall with fiber content. Setup 3, with optimized processing parameters, was the most desirable processing protocol because it allowed the highest fiber fraction (Vf) for the lowest Vp.

Funder

Normandy region and FEDER

Publisher

MDPI AG

Subject

General Materials Science

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