Visible-Light-Photocatalyzed C5-H Nitration of 8-Aminoquinoline Amides-Reference-Cited by-同舟云学术

Visible-Light-Photocatalyzed C5-H Nitration of 8-Aminoquinoline Amides

Published:2024-04-15 Issue:4 Volume:14 Page:263
ISSN:2073-4344
Container-title:Catalysts
language:en
Short-container-title:Catalysts

Author:

Liu Pugen¹,Qiao Huijie¹,Su Xiaoxue¹,Bai Peirong¹,Yang Fan¹

Affiliation:

1. Henan Key Laboratory of Chemical Biology and Organic Chemistry, Key Laboratory of Applied Chemistry of Henan Universities, Green Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou 450052, China

Abstract

A mild and efficient protocol for visible-light-photocatalyzed C5 nitration of 8-aminoquinoline derivatives was developed utilizing Cu(NO3)2∙3H2O as a nitro source. The reaction proceeded smoothly under very mild conditions, employing Acid Red 94 and a commercial household light bulb as an organic photosensitizer and a light source, respectively, making this synthetic procedure green and easy to operate. Furthermore, most products could be obtained through recrystallization, which enhanced the operational simplicity of this method.

Funder

National Natural Science Foundation of China

Publisher

MDPI AG

Link

https://www.mdpi.com/2073-4344/14/4/263/pdf

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