Synthesis of Composite Titanate Photocatalyst via Molten Salt Processing and Its Enhanced Photocatalytic Properties

Abstract

Photocatalysis plays a pivotal role in environmental remediation and energy production and improving the efficiency of photocatalysts, yet enhancing its efficiency remains a challenge. Titanate has been claimed to be a very promising material amongst various photocatalysts in recent years. In this work, a novel composite photocatalyst of sodium titanate and potassium titanate was synthesized via a simple hydrothermal and molten salt calcination method. Low melting point nitrate was added in the calcination process, which helps reduce the calcination temperature. The as-prepared composite sample showed excellent photocatalytic performance compared with commercial P25 in the visible light range. According to the characterization of XRD, SEM, TEM, BET, UV–Vis, and photocatalytic property testing, the composite’s photocatalytic performance results are due to the dual optimization brought about by the layered structure and composite of titanium salts forming a heterojunction. We believe that the composite has significant application potential for the use of titanate in the field of photocatalysis. Notably, this study employed well-documented synthesis methods and adhered to established protocols for experimental procedures.