Optimization of Process Parameters for Preparing Metallic Matrix Diamond Tool Bits by Microwave Pressureless Sintering Using Response Surface Methodology

Author:

Yang Li,Wang Liang,Gao Jiyun,Guo ShenghuiORCID,Ye Xiaolei,Koppala Sivasankar,Hu Tu,Hou Ming,Hu Longtao

Abstract

The process of preparing metallic matrix diamond tool bits by microwave pressureless sintering (MPS) was exclusively studied in this paper. The effects of the sintering temperature, the cold pressure, and the holding time on the mechanical properties of the bit were determined by using the response surface methodology (RSM) with Box-Behnken Design (BBD). In addition, with RSM, the second-order polynomial equation of mechanical properties was obtained. The solutions were well matched with the experimental values. This indicates that major variations in mechanical properties of the sintered sample could be predicted by the models, which shows that the applied model is accurate. Conventional pressureless sintering (CPS) experiments were also conducted to make a comparison. The experimental results showed that the MPS can enhance the mechanical properties of sintered samples. A possible MPS mechanism is proposed in this work after analyzing all the experimental results.

Funder

National Natural Science Foundation of China

Publisher

MDPI AG

Subject

General Materials Science

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