Effect of Process Parameters on Superelasticity of LPBF Ni-Rich Ni51.3Ti48.7 Shape Memory Alloy

Author:

Xiang Zheng1,Yang Qin1,Zhang Tianhao1,Shen Xianfeng1,Chen Jie1,Huang Shuke1

Affiliation:

1. Institute of Machinery Manufacturing Technology, China Academy of Engineering Physics, Mianyang 621000, China

Abstract

Laser powder bed fusion (LPBF) presents both opportunities and challenges with regard to the customisation of NiTi alloy properties. This paper presents a systematic study of the influence of process parameters on the superelasticity of LPBF Ni-rich Ni51.3Ti48.7 shape memory alloy. The findings demonstrate that NiTi alloys produced through disparate process parameters exhibit disparate phase transformation behaviours and microstructures, which in turn result in varying degrees of superelasticity. At an energy density of 166.7 to 233.3 J/mm3, LPBFed Ni-rich Ni51.3Ti48.7 is predominantly in the martensite phase at room temperature due to the high phase transition temperature caused by a large amount of Ni evaporation loss, and exhibits almost no superelasticity. At an energy density of 66.7 to 116.7 J/mm3, LPBFed Ni-rich Ni51.3Ti48.7 has less Ni evaporation loss and lower phase transition temperature. It is primarily austenite phase at room temperature, and contains nano-precipitated phases internally, thereby exhibiting excellent superelasticity. The recovery rate is in excess of 5.5% at the initial compression (up to 5.7%) and in excess of 5.0% following ten cycles (up to 5.3%). Furthermore, the lower the energy density, the smaller the stress–strain hysteresis of LPBFed Ni-rich Ni51.3Ti48.7, with a variation range of 1.8–3.9 mJ/mm3.

Funder

NSAF

Publisher

MDPI AG

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