Advancing Sustainable Wastewater Treatment Using Enhanced Membrane Oil Flux and Separation Efficiency through Experimental-Based Chemometric Learning

Author:

Usman Jamilu1ORCID,Abba Sani I.1,Muhammed Ibrahim2,Abdulazeez Ismail1ORCID,Lawal Dahiru U.1ORCID,Yogarathinam Lukka Thuyavan1ORCID,Bafaqeer Abdullah3ORCID,Baig Nadeem1ORCID,Aljundi Isam H.14ORCID

Affiliation:

1. Interdisciplinary Research Centre for Membranes and Water Security, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi Arabia

2. Department of Chemistry, Faculty of Science, Sokoto State University, Sokoto 852101, Nigeria

3. Center for Refining and Advanced Chemicals, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi Arabia

4. Department of Chemical Engineering, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi Arabia

Abstract

Efficient oil–water separation using membranes directly aligns with removing oil pollutants from water sources, promoting water quality. Hence, mitigating environmental harm from oil spills and contamination and fostering ecosystem health for sustainable development. Computational learning, such as artificial intelligence (AI), enhances membrane oil flux and separation efficiency by optimizing process parameters, leading to improved oil–water separation and aligning AI with sustainable environmental protection and resource efficiency solutions. This study employed phase-inversion coupled with sintering to create the ceramic membrane. The Stöber method was adopted to prepare the superhydrophobic silica sol-gel solutions. The data from the mentioned experiment were imposed into regression models, namely, multilinear regression analysis (MLR), support vector regression (SVR), and robust linear regression (RLR), to simulate three different scenarios (oil flux, separation efficiency, and oil flux and separation efficiency). The outcomes were validated and evaluated using several statistical (R2, MSE, R, and RMSE) and graphical visualizations. For oil flux, the results show that the most effective simulation was achieved in SVR-M2 and the statistical criteria for the testing phase were R2 = 0.9847, R = 0.9923, RMSE = 0.0333, and MSE = 0.0011. Similarly, SVR-M2 was superior to other modeling techniques for the separation efficiency in the testing phase (R2 = 0.9945, R = 0.9972, RMSE = 0.0282, MSE = 0.0008). Reliability outcomes promise to revolutionize how we model and optimize membrane-based oil–water separation processes, with implications for various industries seeking sustainable and efficient solutions.

Funder

Deanship of Research Oversight and Coordination (DROC) at King Fahd University of Petroleum and Minerals (KFUPM) under the Interdisciplinary Research Center for Membranes and Water Security

Publisher

MDPI AG

Subject

Water Science and Technology,Aquatic Science,Geography, Planning and Development,Biochemistry

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