An Investigation of Microstructure Characteristic and Sulfide Stress Cracking Behavior of 110 ksi Cr-Mo Grade Casing Steel

Author:

Lu Caihong12,Zhang Hui1,Li Dening3,Han Lihong2,Wang Jianjun2,Li Jun1,Qi Yue14,Li Fangpo2,Tian Yudong14

Affiliation:

1. College of Petroleum Engineering, China University of Petroleum-Beijing, Beijing 102249, China

2. State Key Laboratory of Performance and Structural Safety for Petroleum Tubular Goods and Equipment Materials, Tubular Goods Research Institute of CNPC, Xi’an 710077, China

3. Tianjin Gas Storage Branch, PetroChina Dagang Oilfield Company, Tianjin 300280, China

4. Drilling Engineering Technology Research Institute of Daqing Drilling Engineering Company, Petrochina Daqing Oilfield Company, Daqing 163413, China

Abstract

The sulfide stress cracking (SSC) behavior of three micro-alloying 110 ksi grade Cr-Mo casing steels were evaluated according to the A-Method tensile test specified in the NACE TM0177 standard (NACE A-method). The fractures of SSC specimens and the micro-structures of the casing steels were characterized by scanning electron microscopy (SEM) with electron backscattering diffraction (EBSD) and transmission electron microscopy (TEM) in the BF and STEM mode. The results show that on the premise of 110 ksi, the yield strength of Co-Mo steel was satisfactory, finer spherical carbides increased the number of irreversible traps; widened polygonised martensitic laths, lowered dislocation density, and lowered the proportion of high-angle grain boundaries and the Σ3 boundaries decreased hydrogen permeability and diffusivity. The SSC resistance of Co-Mo steel with above micro structure characteristics was enhanced.

Funder

China National Petroleum Corporation

Study on Key Technologies of Petroduction Increase and Transformation of Gulong Shale Oil

Innovative Talents Promotion Plan-Young Science and Technology Star Project

Publisher

MDPI AG

Subject

Process Chemistry and Technology,Chemical Engineering (miscellaneous),Bioengineering

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4. Function of hydrogen in embrittlement of high-strength steels;Nagumo;ISIJ Int.,2001

5. Effect of microstructure on the strength of 25CrMo48V martensitic steel tempered at different temperature and time;Zhang;Mater. Des.,2012

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