Infrared Spectroscopy for the Quality Control of a Granular Tebuthiuron Formulation

Author:

Johnson Joel B.ORCID,Farquhar Hugh,Ismay Mansel,Naiker Mani

Abstract

Tebuthiuron is a selective herbicide for woody species and is commonly manufactured and sold as a granular formulation. This project investigated the use of infrared spectroscopy for the quality analysis of tebuthiuron granules, specifically the prediction of moisture content and tebuthiuron content. A comparison of different methods showed that near-infrared spectroscopy showed better results than mid-infrared spectroscopy, while a handheld NIR instrument (MicroNIR) showed slightly improved results over a benchtop NIR instrument (Antaris II FT-NIR Analyzer). The best-performing models gave an R2CV of 0.92 and RMSECV of 0.83% w/w for moisture content, and R2CV of 0.50 and RMSECV of 7.5 mg/g for tebuthiuron content. This analytical technique could be used to optimise the manufacturing process and reduce the costs of post-manufacturing quality assurance.

Publisher

MDPI AG

Subject

General Earth and Planetary Sciences

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