Investigating the Effect of Thermal Annealing and Changing the Concentration of GO in GO/PVA Nanocomposites on Their Structural, Electrical, and Optical Properties

Author:

Gahramanli Lala12ORCID,Muradov Mustafa1,Eyvazova Goncha1,Baghirov Mahammad Baghir1,Mammadyarova Sevinj1,Aliyeva Gunel1,Hajiyev Elman3,Mammadov Faig4,Bellucci Stefano2ORCID

Affiliation:

1. Nano Research Laboratory, Baku State University, 23 Academik Zahid Khalilov Street, Baku AZ 1148, Azerbaijan

2. INFN—Laboratori Nazionali di Frascati, Via E. Fermi 54, 00044 Frascati, Italy

3. Institute of Physics, Azerbaijan National Academy of Science, H. Javid av. 131, Baku AZ 1143, Azerbaijan

4. Institute of Catalysis and Inorganic Chemistry, Azerbaijan National Academy of Science, H. Javid av.131, Baku AZ 1143, Azerbaijan

Abstract

The present research involves producing graphene oxide (GO) using the Hummers method, generating a composite using GO and PVA, and analyzing these composites’ structural and optical characteristics. PVA and GO were used in varied percentages to deal with the issue of how the features of GO/PVA alter depending on concentration. The impact of thermal annealing on the structure and optical characteristics of GO/PVA materials at various concentrations were also investigated. UV-VIS was used to investigate the band gap value of GO/PVA composites. The band gap value changed due to an increase in the concentration of GO in the composites in the PVA and the impact of thermal annealing. The band gap value, specific resistance, and dielectric constant were all found to be well controlled by varying the thermal annealing temperature and the concentration of GO in this case. Differential Scanning Calorimetry (DSC) and thermogravimetric analysis (TGA) were performed on pure PVA and GO/PVA samples in various percentages of GO in order to examine the effect of temperature on the physical properties of (n = 1, 2, 3, 5, 20%) nGO%/PVA nanocomposites. Thermal stability increased as the fraction of GO in the PVA polymer matrix increased.

Publisher

MDPI AG

Subject

General Energy,General Engineering,General Chemical Engineering

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