FT-Raman Methodology Applied to Study the Effect of Time and Type of Seasoning in the Crafting of Sherry Casks® Used in the Aging of Brandy De Jerez

Author:

Guerrero-Chanivet María12ORCID,Guillén-Sánchez Dominico A.1ORCID,Valcárcel-Muñoz Manuel José2ORCID,García-Moreno M. Valme1ORCID,Anjos Ofelia34ORCID

Affiliation:

1. Departamento de Química Analítica, Facultad de Ciencias, Instituto de Investigación Vitivinícola y Agroalimentaria (IVAGRO), Campus Universitario de Puerto Real, Universidad de Cádiz, 11510 Puerto Real, Spain

2. Bodegas Fundador S.L.U., C/San Ildefonso, n 3, 11403 Jerez de la Frontera, Spain

3. CERNAS-IPCB, Research Centre for Natural Resources, Environment and Society, Polytechnic Institute of Castelo Branco, 6001-909 Castelo Branco, Portugal

4. Centro de Biotecnología de Plantas da Beira Interior, 6001-909 Castelo Branco, Portugal

Abstract

Brandy de Jerez is a grape-derived spirit produced in Southern Spain with specific characteristics that come from the casks where it is produced, which must have previously contained some type of Sherry wine for at least 12 months. These casks are known as Sherry Cask®. In this work, Brandies de Jerez aged for different aging times (0, 3, 6 and 12 months) in casks seasoned with three different types of Sherry wines (Fino, Oloroso and Amontillado) have been studied. The samples have been analyzed using FT-Raman spectroscopy, and their chemical characterization has also been realized by studying their total content of organic acid, volatile compounds, and phenolic and furanic compounds. Their chemical study showed that the main differences between the studied samples were due to the duration and the type of seasoning performed. However, the spectra obtained through FT-Raman presented noticeable differences according to cask seasoning time and the Sherry wine used for the process. A PCA (Principal Component Analysis) confirmed that the Brandies de Jerez presented significant differences depending on the seasoning time and type that the casks were subjected to. A PLS-R (Partial Least Squares Regression) study enabled establishing a close correlation between specific regions of the FT-Raman spectra and cask seasoning time.

Funder

niversity of Cadiz and Bodegas Fundador

Publisher

MDPI AG

Subject

Electrical and Electronic Engineering,Biochemistry,Instrumentation,Atomic and Molecular Physics, and Optics,Analytical Chemistry

Reference40 articles.

1. Consejería de Agricultura Pesca y Desarrollo Rural (2018). Orden de 28 de Junio de 2018, por la que se Aprueba el Expediente Técnico de Indicación Geográfica «Brandy de Jerez», Boletín Oficial de la Junta de Andalucía.

2. (2023, October 28). The European Parliament and the Council of the European Union Regulation (EU) 2019/787 On the Definition, Description, Presentation and Labelling of Spirit Drinks, the Use of the Names of Spirit Drinks in the Presentation and Labelling of Other Foodstuffs, the Protection of Geographical Indications for Spirit Drinks, the Use of Ethyl Alcohol and Distillates of Agricultural Origin in Alcoholic Beverages, and Repealing Regulation (EC) No 110/2008; European Union, 2019; p. L130/1-L130/54. Available online: https://eur-lex.europa.eu/legal-content/EN/TXT/?uri=CELEX%3A32019R0787.

3. Valcárcel-Muñoz, M.J., Guerrero-Chanivet, M., García-Moreno, M.V., Rodríguez-Dodero, M.C., and Guillén-Sánchez, D.A. (2021). Comparative Evaluation of Brandy de Jerez Aged in American Oak Barrels with Different Times of Use. Foods, 10.

4. (2023, August 08). Regulatory Council Envinado (Wine-Seasoning) Technical Specifications. Available online: https://www.sherry.wine/documents/87/especificacion_tecnica_de_envinado_rev_03.pdf.

5. Valcárcel-Muñoz, M.J., Guerrero-Chanivet, M., Rodríguez-Dodero, M.C., García-Moreno, M.V., and Guillén-Sánchez, D.A. (2022). Analytical, Chemometric and Sensorial Characterization of Oloroso and Palo Cortado Sherries during Their Ageing in the Criaderas y Solera System. Foods, 11.

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