Facile Synthesis and Characterization of TiO2/SnS Nanocomposites by Eco-Friendly Methods

Author:

Bronusiene Asta1ORCID,Kleinauskas Ricardas1,Ancutiene Ingrida1ORCID

Affiliation:

1. Department of Physical and Inorganic Chemistry, Kaunas University of Technology, Radvilenu Str. 19, LT-50254 Kaunas, Lithuania

Abstract

The acid etching mechanism of FTO film using zinc powders has been explored, and sulfuric and hydrochloric acid solutions of different concentrations were tested as etching agents. Compact and mesoporous films of titanium dioxide were prepared by spin-coating and doctor blade techniques on FTO glass. Tin sulfide films were formed through a successive ionic layer adsorption and reaction (SILAR) process using different numbers of deposition cycles, and TiO2/SnS nanocomposites were synthesized. The thin films and the prepared composites were characterized using X-ray diffraction, UV-Vis spectroscopy, scanning electron microscopy and energy-dispersive X-ray spectroscopy analyses. In this study, the principal characteristics of deposited tin sulfide films on two different types of TiO2 films are shown.

Publisher

MDPI AG

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