(R)-(+)-3,5-Dinitro-N-(1-phenylethyl)benzothioamide-Reference-Cited by-同舟云学术

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(R)-(+)-3,5-Dinitro-N-(1-phenylethyl)benzothioamide

Published:2023-05-20 Issue:2 Volume:2023 Page:M1650
ISSN:1422-8599
Container-title:Molbank
language:en
Short-container-title:Molbank

Author:

Donahue Matthew G.¹^ORCID,Crull Emily¹

Affiliation:

1. Department of Chemistry and Biochemistry, University of Southern Mississippi, Hattiesburg, MS 39406, USA

Abstract

(R)-(+)-3,5-dinitro-N-(1-phenylethyl)benzothioamide 1 is a potential chiral solvating agent (CSA) for the spectral resolution of enantiomers via 1H NMR spectroscopy. The single enantiomer of 1 was synthesized from commercially available (R)-(+)-a-methylbenzylamine 2 in two steps with 85% yield.

Funder

NIGMS

NSF

Publisher

MDPI AG

Subject

Organic Chemistry,Physical and Theoretical Chemistry,Biochemistry

Link

https://www.mdpi.com/1422-8599/2023/2/M1650/pdf

Reference25 articles.

1. Silva, M.S. (2017). Recent Advances in Multinuclear NMR Spectroscopy for Chiral Recognition of Organic Compounds. Molecules, 22.

2. Chiral Reagents for the Determination of Enantiomeric Excess and Absolute Configuration Using NMR Spectroscopy;Wenzel;Chirality,2003

3. Gal, J. (2013). Differentiation of Enantiomers I, Springer.

4. NMR Determination of Enantiomeric Purity;Parker;Chem. Rev.,1991

5. A Convenient Family of Chiral Shift Reagents for Measurement of Enantiomeric Excesses of Sulfoxides;Deshmukh;Tetrahedron Lett.,1984

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