1-(2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2-oxoethyl) Quinolin-1-ium Bromide-Reference-Cited by-同舟云学术

1-(2-(3,5-Di-tert-butyl-4-hydroxyphenyl)-2-oxoethyl) Quinolin-1-ium Bromide

Published:2024-01-24 Issue:1 Volume:2024 Page:M1763
ISSN:1422-8599
Container-title:Molbank
language:en
Short-container-title:Molbank

Author:

Rusew Rusi¹^ORCID,Iliev Kostadin¹,Kurteva Vanya²^ORCID,Shivachev Boris¹^ORCID

Affiliation:

1. Institute of Mineralogy and Crystallography “Acad. Ivan Kostov”, Bulgarian Academy of Sciences, Acad. G. Bonchev Street, bl. 107, 1113 Sofia, Bulgaria

2. Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences, Acad. G. Bonchev Street, bl. 9, 1113 Sofia, Bulgaria

Abstract

The title compound 1-(2-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-oxoethyl) quinolin-1-ium bromide was obtained in good yield by a facile one-pot, one-step synthetic procedure involving quinoline and an aromatic α-bromo ketone. The product was isolated using hot recrystallization from acetone/acetonitrile solution and characterized using powder and single-crystal XRD, 1D and 2D NMR, DSC, FT-IR, and HRMS analyses.

Funder

Bulgarian National Science Fund

Publisher

MDPI AG

Link

https://www.mdpi.com/1422-8599/2024/1/M1763/pdf

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