Optimizing DMF Utilization for Improved MXene Dispersions in Epoxy Nanocomposites

Author:

Janjua Ayyaz Ali1,Younas Muhammad1,Ilyas Rushdan Ahmad2ORCID,Shyha Islam3,Faisal Nadimul Haque1ORCID,Inam Fawad45,Saharudin Mohd Shahneel1ORCID

Affiliation:

1. School of Engineering, Robert Gordon University, Aberdeen AB10 7GE, UK

2. Department of Chemical Engineering, Faculty of Chemical and Energy Engineering, Universiti Teknologi Malaysia, Skudai 81310, Malaysia

3. School of Computing, Engineering and Built Environment, Edinburgh Napier University, 10 Colinton Road, Edinburgh EH10 5DT, UK

4. School of Architecture, Computing and Engineering, University of East London, London E16 2RD, UK

5. Executive Principal Office, Oxford Business College, 23-38 Hythe Bridge Street, Oxford OX1 2EP, UK

Abstract

Dimethylformamide (DMF), a polar solvent, is commonly used for preparing graphene/epoxy nanocomposites. While previous research has commonly predominantly highlighted the improvement in physio-mechanical properties of these nanocomposites, the effect of DMF on processing and its direct influence on the final characteristics of MXene/epoxy nanocomposites have not been investigated. This unexplored link between DMF dosage, MXene concentrations, and the final composite properties presents an exciting direction for future research. In this study, a fixed dosage of DMF was used with varying MXene concentrations to fabricate the nanocomposites. To assess the reliability of DMF dosage on the characteristics of the fabricated nanocomposites, various evaluation techniques were employed, including dispersion evaluation, mechanical tests, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), scanning electron microscopy (SEM), electromagnetic interference (EMI) shielding, and surface roughness measurements. The research outcomes revealed that as MXene concentration increased, the characteristics of the MXene/epoxy nanocomposites, improved across the board, indicating their potential for use in energy storage applications.

Funder

Carnegie Trust for the Universities of Scotland

Publisher

MDPI AG

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