Rietveld Refinement, Structural Characterization, and Methylene Blue Adsorption of the New Compound Ba0.54Na0.46Nb1.29W0.37O5

Author:

Es-soufi HichamORCID,Bih HssainORCID,Bih Lahcen,Rajesh RamanORCID,Lima Alan Rogerio FerreiraORCID,Sayyed M. I.,Mezher RabihORCID

Abstract

Using the solid-state process, the new compound Ba0.54Na0.46Nb1.29W0.37O5 was effectively produced in a single crystalline phase. The material’s characteristics were determined by X-ray diffraction and Raman techniques. The Rietveld method was applied to refine the structural properties of this sample using X-ray diffraction data and derive the diffraction line profile. The cell parameters a = b = 12.37843 ± 0.02 and c = 3.93526 ± 0.02 were accustomed to crystallizing this compound in the tetragonal tungsten bronze (TTB) structure of the space group P4bm. Thanks to Raman measurements, we were able to detect numerous vibration modes in this crystalline phase. The adsorption of methylene blue (MB) on crystalline phase was studied by UV–visible spectroscopy. On account of methylene blue adsorption on Ba0.54Na0.46Nb1.29W0.37O5, it was discovered that this material can be used to remove organic pollutants and thus be used for water treatment.

Publisher

MDPI AG

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science,General Chemical Engineering

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