The Changing of Micromechanical Properties of Coal after Water Immersion: The Insight from Nanoindentation Test

Abstract

The application of the hydrodynamic method has enhanced the extraction of coal bed methane (CBM). In this method, fracturing fluid rapidly penetrates the coal reservoir, altering its intrinsic pore structure and microscopic mechanical properties. These changes impact the properties of the coal reservoir and CBM depletion. It is, therefore, crucial to explore how these micro-characteristics evolve following water invasion. In this context, using nanoindentation tests, the microscopic characteristics of three coal samples were measured under dry conditions and at water saturations corresponding to 44% and 75% relative humidity. The influence of water immersion on the pore structure was also assessed using mercury injection experiments. Moreover, cluster analysis was used to categorize the extensive measured data into three sub-components: fractures (large pores), inertinite, and vitrinite, to investigate the impact of water saturation on microscopic properties. The findings indicate that cluster analysis is well-suited to these data, showing excellent agreement with porosity and maceral tests. The relationship between the elastic modulus and hardness of dry and wet coal samples varies across the sub-components. There is a notable dependency in the case of vitrinite, whereas water content tends to reduce this dependency. It is also found that water content negatively affects elastic modulus and hardness and reduces the anisotropy ratio. The mechanical properties of inertinite are highly responsive to water immersion, whereas vitrinite exhibits lesser sensitivity. The softening mechanisms of coal when immersed in water, such as calcite phase dissolution, swelling stress fracturing, and weakening of macerals, are identified. This study offers new perspectives on the impact of moisture on the alteration of micromechanical properties in coal.