Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF

Author:

Lu Yuxian12,Zhang Hao1,Xue Peng1,Wu Lihui1,Liu Fengchao1,Jia Luanluan3,Ni Dingrui1,Xiao Bolv1,Ma Zongyi1

Affiliation:

1. Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

2. School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China

3. Shandong Key Laboratory of Advanced Aluminum Materials and Technology, Binzhou Institute of Technology, Weiqiao—UCAS Science and Technology Park, Binzhou 256606, China

Abstract

Laser powder bed fusion (LPBF) is a typical additive manufacturing technology that offers significant advantages in the production of complex components. With the rapid heating and cooling characteristics of LPBF, a large amount of solid solution of alloying elements in the matrix can be achieved to form supersaturated solid solutions, thus enhancing the properties of LPBF alloys. For the unique microstructure, the heat treatment process needs to be adjusted accordingly. In this work, a Zr/Sc-modified Al-Mg alloy processed by laser powder bed fusion (LPBF) with relatively low cost and good mechanical properties was investigated. The fine microstructure was obtained under rapid solidification conditions. The nanoscale Al3(Sc,Zr) particles precipitated at the molten pool boundary during solidification. These particles, as effective heterogeneous nucleators, further refined the α-Al grains and improved the mechanical properties of the alloy. As a result, the alloy exhibited a heterogeneous microstructure consisting of columnar grains in the center of the molten pool and equiaxed grains at the boundaries. The rapid solidification resulted in the supersaturation of solute atoms in the α-Al matrix, which significantly enhanced the solid solution strengthening effect. With the LPBF processing parameters of a combination of a laser power of 250 W, a laser scanning speed of 833 mm/s, and stripe scanning mode, the tensile strength of the alloy reached 401.4 ± 5.7 MPa, which was significantly higher than that of the cast alloys with aging treatment (281.1 ± 1.3 MPa). The heat treatment promoted the formation of secondary Al3(Sc,Zr), Mn/Mg-rich phases. The ultimate tensile strength and elongation at fracture after aging at 325 °C for 2 h were 536.0 ± 1.7 MPa and 14.8 ± 0.8%, respectively. The results provide insight into the preparation of aluminum alloys with relatively low cost and excellent mechanical properties.

Funder

National Key Research and Development Program of China

National Natural Science Foundation of China

Youth Innovation Promotion Association, CAS

Bintech-IMR R&D Program

Publisher

MDPI AG

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science,General Chemical Engineering

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