Design of Titanium Alloys Insensitive to Thermal History for Additive Manufacturing

Author:

Ueda Masato12,Ting Hsuan Chang3,Ikeda Masahiko4,Nakano Takayoshi5ORCID

Affiliation:

1. Department of Chemistry and Materials Engineering, Faculty of Chemistry, Materials and Bioengineering, Kansai University, 3-3-35, Yamate-cho, Suita 564-8680, Japan

2. Carbon Neutrality Research Centre, Kansai University, 3-3-35, Yamate-cho, Suita 564-8680, Japan

3. Graduate School of Science and Engineering, Kansai University, 3-3-35, Yamate-cho, Suita 564-8680, Japan

4. Nihon Superior Co., Ltd., 1-16-15 Esaka-Cho, Suita 564-0063, Japan

5. Division of Materials and Manufacturing Science, Graduate School of Engineering, Osaka University, 2-1, Yamadaoka, Suita 565-0871, Japan

Abstract

Powder bed fusion is the most common technology used for 3D printing, where thermal energy is used to selectively melt/sinter granular materials into solid shapes. The build platform is then lowered, more powder is added, and the process is repeated for the next layer to fully print the design. As a result, the built-up part is repeatedly heated. Therefore, materials that are not sensitive to thermal history are preferred for this process. The Ti–Zr system forms a continuous solid solution for both β- and α-phases. The presence of Fe in Ti alloys is inevitable; however, it provides some beneficial effects. The purpose of this work was to prepare Ti–Zr–Fe alloys and investigate their heat treatment behaviour. Ti-xmass%Zr-1mass%Fe alloys (x = 0, 5, 10) were prepared with arc melting. The formation of a solid solution of Zr in Ti was confirmed on the basis of X-ray diffraction peak shifts and hardening effects. A small amount of β-phase precipitation was suggested by the change in electrical resistivity after isothermal ageing at 673 and 773 K. However, no obvious phase or microstructural changes were observed. The laser scanning increased the volume of the precipitates and also coarsened them, but the effect was limited.

Funder

Ministry of Education, Culture, Sports, Science and Technology (MEXT) of Japan

Japan Science and Technology Agency

Publisher

MDPI AG

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science,General Chemical Engineering

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