Studies of Fractal Microstructure in Nanocarbon Polymer Composites

Author:

Artyukov Igor1ORCID,Bellucci Stefano2ORCID,Kolesov Vladimir3ORCID,Levin Vadim4,Morokov Egor45ORCID,Polikarpov Maxim6,Petronyuk Yulia47ORCID

Affiliation:

1. X-ray Optics Laboratory, Lebedev Physical Institute, Russian Academy of Sciences, 119991 Moscow, Russia

2. INFN-Laboratori Nazionali di Frascati, 00044 Frascati, Italy

3. Kotel’nikov Institute of Radio Engineering and Electronics, Russian Academy of Sciences, 125009 Moscow, Russia

4. Laboratory of Acoustic Microscopy, Emanuel Institute of Biochemical Physics, Russian Academy of Sciences, 119334 Moscow, Russia

5. Department of Physics and Mathematics, Pirogov Russian National Research Medical University, 117997 Moscow, Russia

6. European Molecular Biology Laboratory, Hamburg Unit c/o DESY, 22607 Hamburg, Germany

7. Scientific and Technological Center of Unique Instrumentation, Russian Academy of Sciences, 117342 Moscow, Russia

Abstract

The in situ study of fractal microstructure in nanocarbon polymers is an actual task for their application and for the improvement in their functional properties. This article presents a visualization of the bulk structural features of the composites using pulsed acoustic microscopy and synchrotron X-ray microtomography. This article presents details of fractal structure formation using carbon particles of different sizes and shapes—exfoliated graphite, carbon platelets and nanotubes. Individual structural elements of the composite, i.e., conglomerations of the particles in the air capsule as well as their distribution in the composite volume, were observed at the micro- and nanoscale. We have considered the influence of particle architecture on the fractal formation and elastic properties of the composite. Acoustic and X-ray imaging results were compared to validate the carbon agglomeration.

Funder

Ministry of Science and Higher Education of the Russian Federation

Publisher

MDPI AG

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