The Role of 3D Printing in the Development of a Catalytic System for the Heterogeneous Fenton Process

Author:

D’Accolti Lucia1ORCID,De Cataldo Alessia1ORCID,Montagna Francesco2,Esposito Corcione Carola23ORCID,Maffezzoli Alfonso23ORCID

Affiliation:

1. Department of Chemistry, University of Bari, Orabona 4, 70125 Bari, Italy

2. Department of Engineering for Innovation, University of Salento, Arnesano, 73100 Lecce, Italy

3. National Interuniversity Consortium of Materials Science and Technology, University of Salento, Arnesano, 73100 Lecce, Italy

Abstract

Recycling of catalysts is often performed. Additive manufacturing (AM) received increasing attention in recent years in various fields such as engineering and medicine, among others. More recently, the fabrication of three-dimensional objects used as scaffolds in heterogeneous catalysis has shown innumerable advantages, such as easier handling and waste reduction, both leading to a reduction in times and costs. In this work, the fabrication and use of 3D-printed recyclable polylactic acid (PLA) scaffolds coated with an iron oxide active catalyst for Fenton reactions applied to aromatic model molecules, is presented. These molecules are representative of a wider class of intractable organic compounds, often present in industrial wastewater. The 3D-printed PLA-coated scaffolds were also tested using an industrial wastewater, determining the chemical oxygen demand (COD). The catalyst is characterized using electron microscopy coupled to elemental analysis (SEM/EDX) and thermogravimetry, demonstrating that coating leach is very limited, and it can be easily recovered and reused many times.

Funder

MITE

Publisher

MDPI AG

Subject

Polymers and Plastics,General Chemistry

Reference40 articles.

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