Effect of PVDF, HA, and AgNO3 Annealing on β-Phase, Optical, and Mechanical Properties

Author:

Markuniene Ieva1,Palevicius Arvydas1ORCID,Vezys Joris1,Augustyniak Jakub12ORCID,Perkowski Dariusz2ORCID,Urbaite Sigita1ORCID,Janusas Giedrius1ORCID

Affiliation:

1. Faculty of Mechanical Engineering and Design, Kaunas University of Technology, Studentu St. 56, LT 51373 Kaunas, Lithuania

2. Faculty of Mechanical Engineering, Bialystok University of Technology, Wiejska 45 C Street, 15-351 Białystok, Poland

Abstract

Typically, polymer composites and ceramics are used to create biosensors. Materials with properties that are ideal for biosensors and chemical sensors include AgNO3 (silver nitrate), PVDF (polyvinylidene fluoride), and HA (hydroxyapatite). Polyvinylidene fluoride (PVDF) polymer has been widely used in several applications because of its well-known superior ferroelectric characteristics and biocompatibility. The brittleness and low bending strength of hydroxyapatite limit its applicability. Several HA and polymer composite formulations have been developed to compensate for HA’s mechanical weakness. The final product contains a significant amount of HA, making HA/polymer composites highly biocompatible. When the right amount of silver is deposited, the maximum piezoelectric activity is generated, and silver nitrate has antimicrobial properties. The non-toxic solvent DMSO (dimethyl sulfoxide) and the solvent casting method were chosen for the preparation of the film. Surface roughness was chosen to measure the Str and Sdr properties of the thin film. For liquid preparation, the multifractal spectra analysis was chosen for each sample. SEM was used to examine the samples morphologically. EDX and mapping analyses were presented for chemistry distribution in the samples.

Funder

Research Council of Lithuania

Publisher

MDPI AG

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