Design, Implementation, and Characterization of a Compact Lock-in Add-on for Low-Frequency Impedance Measurements

Abstract

Impedance measurements are crucial in a variety of applications, from the characterization of lithium batteries, microbial fuel cells, and biosensors to the study of polymers and material degradation, where strict requirements have to be met in terms of frequency bandwidth and current level. Here, we present a cost-effective compact solution for ultra-low-frequency impedance measurements, operating in a wide range, from 1 mHz to 250 kHz. Coupled to a lock-in amplifier, the designed circuit is based on a Howland current pump cascaded by a precision current divider in order to set the conversion factor at 100 nA/V, 1 μA/V, or 100 μA/V. Therefore, it is possible to generate very low-current signals to measure resistive impedances up to 100 MΩ. In addition, a feedback network is inserted to null the voltage drift induced by leakage currents and offset voltages, thus allowing the measurement of low-capacitance loads, experimentally tested down to 10 nF. Remarkably, the feedback network allows to perform measurements also in the presence of high voltage bias of the load and experimental results performed up to 60 V demonstrate the excellent stability of the designed system, thus a high voltage compliance. The proposed circuit is particularly interesting for the conditioning of both resistive and capacitive sensors and it is likely to be an effective solution for the implementation of a portable instrument for measuring signals from biosensors.