Optimization of Electrical and Mechanical Properties through the Adjustment of Design Parameters in the Wet Spinning Process of Carbon Nanotube/Polyvinylidene Fluoride Fibers Using Response Surface Methodology

Abstract

The optimal process conditions for fabricating carbon nanotube (CNT)/polyvinylidene fluoride (PVDF) fibers with varying properties using a wet spinning process were experimentally determined. A dope solution was prepared using multi-walled nanotubes, PVDF, and dimethylacetamide, and appropriate materials were selected. Design parameters affecting the chemical and physical properties of CNT/PVDF fibers, such as bath concentration, bath temperature, drying temperature, and elongation, were determined using a response surface method. The wet-spinning conditions were analyzed based on the tensile strength and electrical conductivity of the fibers using an analysis of variance and interaction analysis. The optimized process conditions for fabricating CNT/PVDF fibers with different properties were derived and verified through fabrication using the determined design parameters.